Characterisation of bioadhesive protein-PEG conjugates grafted to titanium surfaces

DOI

Summary: Titanium implants are surgically important and require a hydrophilic polymer coating to prevent biofouling in situ. Bioadhesive proteins can be covalently tethered to the polymer to aid implant-tissue integration. It is not known if protein conjugation changes the polymer layer, or what orientation the proteins exist in for cell adhesion. This proposal will characterise these polymer/protein coatings on titanium surfaces. Objectives: 1) Characterise a key bioadhesive protein (FIII9¿10) at the bare titanium surface (control), over various concentrations, with 2 subphase contrasts, determining protein fraction, orientation and surface excess. 2) Characterise the polymeric layer synthesised on the titanium surface in situ before and after covalent conjugation of FIII9¿10, determining polymer layer thickness and density, and protein parameters as in (1).

Identifier
DOI https://doi.org/10.5286/ISIS.E.24079735
Metadata Access https://icatisis.esc.rl.ac.uk/oaipmh/request?verb=GetRecord&metadataPrefix=oai_datacite&identifier=oai:icatisis.esc.rl.ac.uk:inv/24079735
Provenance
Creator Dr Stephen Holt; Dr Chris van der Walle
Publisher ISIS Neutron and Muon Source
Publication Year 2013
Rights CC-BY Attribution 4.0 International; https://creativecommons.org/licenses/by/4.0/
OpenAccess true
Contact isisdata(at)stfc.ac.uk
Representation
Resource Type Dataset
Discipline Photon- and Neutron Geosciences
Temporal Coverage Begin 2010-05-04T07:32:57Z
Temporal Coverage End 2010-05-06T05:00:05Z