Unraveling temperature dependent cis/trans-isomerisation in bis{(trifluoromethyl)sulfonyl}imide ionic liquids and molten salts

DOI

Raman spectroscopy has identified differences in how the anion conformer populations of alkali metal bis{(trifluoromethyl)sulfonyl}imide molten salts (Li-Cs) and protic 1-H-3-methylimidazolium [Hmim][NTf2] ionic liquids evolve with temperature. In the alkali metal systems, the trans-anion population grows with temperature as anticipated, whereas protic imidazolium ionic liquids show an increase in the more constrained cis-conformer. The objective of this work is (i) to examine changes in the anion cis/trans populations with temperature in thetwo systems in order to compare with, and ideally validate, results obtained from Raman spectroscopy data,and (ii) to generate an atomistic (ionic) description of differences in liquid structure, and subsequently cation-anion interaction modes present, with different types of cation.

Identifier
DOI https://doi.org/10.5286/ISIS.E.24091103
Metadata Access https://icatisis.esc.rl.ac.uk/oaipmh/request?verb=GetRecord&metadataPrefix=oai_datacite&identifier=oai:icatisis.esc.rl.ac.uk:inv/24091103
Provenance
Creator Professor John Holbrey; Mr Adam Turner; Dr Vassileios Dracopoulos; Ms Jade McCune; Professor Gosia Swadzba-Kwasny; Dr Sarah Norman; Ms Caithlin White; Dr Fergal Coleman
Publisher ISIS Neutron and Muon Source
Publication Year 2016
Rights CC-BY Attribution 4.0 International; https://creativecommons.org/licenses/by/4.0/
OpenAccess true
Contact isisdata(at)stfc.ac.uk
Representation
Resource Type Dataset
Discipline Photon- and Neutron Geosciences
Temporal Coverage Begin 2013-10-19T08:15:56Z
Temporal Coverage End 2013-10-30T00:00:00Z