Fast in situ nanothermographies of 3D printed structures during a heat treament up to 1000°C for investigating their sintering

DOI

The CEA and the IRCER are interested in the 3D printing of ceramic structures in order to look for innovative heat exchangers applied to the energy transition. The chosen technique is stereolithography, which uses a polymer resin loaded with silica microparticles. To obtain ceramics, a heat treatment is applied to eliminate the organic part and to promote the formation of bridges between microparticles by sintering. In order to ensure the mechanical properties, it is important to control the heat treatment parameters (temperature, speed and heating time) as they influence the final microstructure of the ceramic object. The objective of high resolution tomographic measurements on beamline ID16B is to access the evolution of the microstructure (neck growth at the early stages of sintering) in situ at different times during the application of the heating profile up to 1000°C. This data will help to validate a model of sintering behavior using the discrete element method.

Identifier
DOI https://doi.org/10.15151/ESRF-ES-753380011
Metadata Access https://icatplus.esrf.fr/oaipmh/request?verb=GetRecord&metadataPrefix=oai_datacite&identifier=oai:icatplus.esrf.fr:inv/753380011
Provenance
Creator Alexandre MAITRE ORCID logo; Denis ROCHAIS ORCID logo; Aya BENJIRA; Guy ANTOU; Clement LAUTE; Julie VILLANOVA
Publisher ESRF (European Synchrotron Radiation Facility)
Publication Year 2025
Rights CC-BY-4.0; https://creativecommons.org/licenses/by/4.0
OpenAccess true
Representation
Resource Type Data from large facility measurement; Collection
Discipline Particles, Nuclei and Fields