In situ mapping of crack progression in nanocrystalline FeCr: nanoscale stress-strain evolution in nanocrystalline microstructure

DOI

Although nanocrystalline materials do exhibit outstanding mechanical properties, the underlying correlation between their nanoscopic microstructure with a large volume fraction of grain boundaries and nanoscopic the plasticity-fracture process interactions still remain unclear. Here, in situ nanodiffraction will be used to characterize nanocrystalline supersaturated FeCr alloys machined using FIB as cantilevers during stepwise loading. We aim to follow nanoscopic crack propagation and elasto-plastic deformation using SAXS and to simultaneously assess X-ray elastic strain and texture evolution at the crack tip using WAXS. The experiment will be performed using a dedicated in situ micromechanical stage developed for ID13 and complemented by numerical analysis. The results will uncover the nanoscopic plasticity-fracture process interactions at the crack tip of nanocrystalline FeCr, aiming to better understanding of semi-brittle fracture.

Identifier
DOI https://doi.org/10.15151/ESRF-ES-514138045
Metadata Access https://icatplus.esrf.fr/oaipmh/request?verb=GetRecord&metadataPrefix=oai_datacite&identifier=oai:icatplus.esrf.fr:inv/514138045
Provenance
Creator Jozef KECKES; Michael SZTUCKI ORCID logo; Juraj TODT (ORCID: 0000-0003-3067-798X); Tobias ZIEGELWANGER; Michael MEINDLHUMER ORCID logo
Publisher ESRF (European Synchrotron Radiation Facility)
Publication Year 2024
Rights CC-BY-4.0; https://creativecommons.org/licenses/by/4.0
OpenAccess true
Representation
Resource Type Data from large facility measurement; Collection
Discipline Particles, Nuclei and Fields