Measuring of Dissolved Inorganic Carbon (DIC) with Automated Infra-Red Inorganic Carbon Analyzer (AIRICA)

DOI

Dissolved Inorganic Carbon (DIC) is one of four parameters measured in order to determine the marine carbonate system. The AIRICA system (Serial No. #027, Marianda, Tulpenweg 28, D-24145 Kiel) works by acidifying (2 acid strokes of 10 % phosphoric acid) a discrete sample amount (2100 µL), generating CO2. The carbon is released out of the water with the help of a carrier gas (99,999 % Nitrogen) that streams through the acidified probe (180 ml min-1). The gas flows through a NAFION dryer and Peltier cooler in order to dry the gas stream. The AIRICA system measures the CO2 concentration by using an infrared detector LICOR 7000 (LI-COR Environmental – GmbH, Siemensstrasse 25A, 61352 Bad Homburg, Germany). Once in the LICOR detector, the CO2 generates a peak, whose area is directly proportional the carbon released, allowing DIC concentration to be calculated when the exact amount of the sample is known. With the help of certified reference materials (Reference material for CO2 measurements, University of California, San Diego, Scripps Institution of Oceanography, Marine Physical Laboratory, 9500 Gilman Drive, La Jolla), previously unnoticed blank impurities can be fixed, leading to more precise measurements and more valuable data. A precision of 1.5-2 µmol kg-1 can be reached. In addition, an average of three repeated measurements is determined, with a maximum deviation of 3 µmol kg-1.

Identifier
DOI https://doi.org/10.1594/PANGAEA.931015
Metadata Access https://ws.pangaea.de/oai/provider?verb=GetRecord&metadataPrefix=datacite4&identifier=oai:pangaea.de:doi:10.1594/PANGAEA.931015
Provenance
Creator Otto, Stefan; Müller, Jens Daniel ORCID logo; Rehder, Gregor ORCID logo
Publisher PANGAEA
Publication Year 2021
Funding Reference Bundesministerium für Bildung und Forschung, Bonn https://doi.org/10.13039/501100002347 Crossref Funder ID 03F0773A https://foerderportal.bund.de/foekat/jsp/SucheAction.do?actionMode=view&fkz=03F0773A Integrated carbon and trace gas monitoring for the Baltic Sea
Rights Creative Commons Attribution 4.0 International; https://creativecommons.org/licenses/by/4.0/
OpenAccess true
Representation
Resource Type Dataset
Format text/tab-separated-values
Size 478 data points
Discipline Earth System Research
Spatial Coverage (17.846W, 59.483S, 25.015E, 65.535N)
Temporal Coverage Begin 2019-02-28T00:00:00Z
Temporal Coverage End 2019-03-11T00:00:00Z