In the search for suitable materials for applications in energy storage, properties such as capacity and cycling stability are of great importance in pushing battery technology forward and meeting the increasing demands for renewable energy applications. This experiment aims to study the promising high capacity material LixVO2F and structural related changes in the material to better understand how these influences the capacity and cycling stability. As for now, the structure of the material during electrochemical cycling is not well understood. A better understanding of the structural properties of the material is necessary to make improvements in the electrochemical performance related to energy storage.